Synthesis and structural characterization of CsNiP crystal

[摘要] CsNiP crystals were synthesized by hydrothermal technique and characterized by the X-ray diffraction method. This alkaline transition metal phosphide crystallizes in the hexagonal system with space group P6$_3/mmc$ and cell parameters, ð‘�? = 7.173(2) Ã�?, ð‘�? = 5.944(9) Ã�?, ð‘�?? = 264.87(7) Ã�?³ and ð‘�? = 2. The final residual factor is ð‘�??1 = 0.0362 for 206 reflections with 𝐼 > 2𝜎(𝐼).

[学科分类] 材料工程

[关键词] Phosphides;hydrothermal;crystal structure;FTIR;DTA.